Hokkaido University Research Profiles

Japanese
Nanotechnology / Materials

Microscopic Indentation

Visualization of hardness/deformation in small areas

We have enabled the in-situ observation of changes in indentation shapes and surrounding surfaces during indentation hardness tests. This will contribute to material development and the clarification of causes of accidents through the high-throughput collection of accurate data enabled by the combination of high temporal resolution of information from video recording and hardness tests.

Content of research

The hardness test, a method to clarify the strength of materials from the deformation caused by local loading, is widely used based on its high simplicity and reproducibility. To obtain highly accurate stress response information while taking advantage of the simplicity of this method, we have developed in-situ hardness tests (micro-indentation) method.
To observe the surface of the specimen both inside and around the indentation through a transparent indenter during the indentation test, it is necessary to optimize the optical conditions. However, by introducing a liquid with a refractive index close to that of the transparent indenter around the indenter, we have enabled a wide range of surface observations.

  • Fig. Results of loading/unloading observations of NiTi superelastic alloy

Potential for social implementation

  • ・Clarification and screening of pseudo-plastic deformation behavior of superelastic NiTi alloy by Brinell indenter.
  • ・Introduction of deformation twinning in magnesium alloys around a Brinell indenter.
  • ・Direct observation of the crack propagation process with a Vickers indenter.

Appealing points to industry and local governments

This invention is a simple system that can be used not only for basic research but also for product management. It is the result of our joint research with AIST, Tokyo Institute of Technology and Hirosaki University. For inquiries, please contact the Institute for the Promotion of Business-Regional Collaboration.

Intellectual property related to this research

特願2016-210069 「圧子透過式試験体表面観察装置、観察方法及び動画像解析・装置制御・特性値演算用プログラム」
2022/5/27Released